TA Instruments

75% SIH 25% PCHINA-0037f

06/05/2022 11:26:05 a. m.

Sample name	25% SIH 75% PCHINA
Sample notes	 
Experiment notes	
Operator	
Sample density	1,000 g/cm^3
Results file name	25% SIH 75% PCHINA
Run number	37 
Results directory	C:\Ta\Data\Ar1500\Ar1500\DIEGO ROA
Experiment was run on	06/05/2022 11:26:05 a. m.

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 1
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 2
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 3
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 4
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Conditioning Step 2
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	10,00 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Temperature ramp step 1
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	25,0 C
End temperature	90,0 C
Wait for start temperature	Yes
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 2
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	90,0 C
Wait for start temperature	No
Ramp duration	0:05:00 hh:mm:ss
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Temperature ramp step 3
Step notes	
Perform step	Yes
Ramp type	Temperature ramp
Start temperature	90,0 C
End temperature	25,0 C
Wait for start temperature	No
Ramp rate	10,00 C/min
Delay time	0:00:09 hh:mm:ss
Controlled variable	shear rate 10,00 1/s
Motor mode	auto 

Step name	Conditioning Step 3
Step notes	
Perform step	Yes
Initial temperature	25,0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Perform pre-shear	Yes
Pre-shear variable	1,000 1/s
Pre-shear duration	0:00:10 hh:mm:ss
Motor mode	auto 
Perform equilibration	Yes
Equilibration duration	0:02:00 hh:mm:ss
Wait for zero velocity	No
Purge gas only	No

Step name	Stepped flow step 5
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000E-3 1/s
End controlled variable	shear rate 0,01000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 6
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,01000 1/s
End controlled variable	shear rate 0,1000 1/s
Ramp mode	log 
Points per decade	3 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 7
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 0,1000 1/s
End controlled variable	shear rate 1,000 1/s
Ramp mode	log 
Points per decade	5 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Stepped flow step 8
Step notes	
Perform step	Yes
Ramp type	Stepped flow
Start controlled variable	shear rate 1,000 1/s
End controlled variable	shear rate 100,0 1/s
Ramp mode	log 
Points per decade	8 
Temperature	25,0 C
Wait for temperature	No
Constant time	0:00:10 hh:mm:ss
Average last x seconds	0:00:05 hh:mm:ss
Motor mode	auto 
Integer rotation averaging	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	No
Set temperature system idle	No

Geometry name	Starch cell
Geometry notes	Starch cell
Geometry material	High temperature
gap	5500 micro m
Calibration factor	10800 
Gap offset	0 micro m
Geometry inertia	2,226 micro N.m.s^2
Shear rate factor	1,000 
Shear stress factor	10800 1/m^3
Measurement system factor	10800 1/m^3
Fluid density factor	1,000E-15 m^5
Normal force factor	1,000 1/m^2
Backoff distance	1,25E5 micro m

Gap zero mode	Standard
Sample compression	none 
Compression distance	1000,0 micro m
Compression velocity	100,0 micro m/s
Fine velocity	1000,0 micro m/s
Coarse velocity	3000,0 micro m/s
Other velocity	3000,0 micro m/s
Current temperature system	Starch cell
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	5,0 C
Cooling water range	15,0 C
Bearing friction correction	Yes
Bearing friction	1,222 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1,0000 , offset 0 C
	Water bath - span 1,0000 , offset 0 C
	Torsion oven - plate - span 1,0000 , offset 0 C
	Torsion oven - solid sample - span 1,0000 , offset 0 C
	Peltier concentric cylinders - span 1,0000 , offset 0 C
	None - span 1,0000 , offset 0 C
	Stress relaxation - span 1,0000 , offset 0 C
	Current temperature system - span 1,0000 , offset 0 C
Bearing mapping type	fast 
Number of mapping iterations	1
Instrument type (MType)	AR1500ex
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	172.23.191.2
Software version	V5.8.2
Windows version	Windows XP 6.2
Instrument inertia	15,97 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0,2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0,1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	3,000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	No
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	No
Creep zero displacement	Yes
Store images to the results for creep steps	No
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	No
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	No
Flow torque limit	10,00 micro N.m
Flow velocity limit	1,000E-3 rad/s
Oscillation torque limit	5,00 micro N.m
Oscillation displacement limit	1,00E-5 rad
Oscillation raw phase limit	170,0 degrees
Oscillation minimum normal force limit	0 N
Oscillation maximum normal force limit	0 N
Flow velocity tolerance	5,00 %
Oscillation torque tolerance	1,00 %
Oscillation displacement tolerance	5,00 %
Oscillation velocity tolerance	5,00 %
Temperature tolerance	1,0 C

Stepped flow step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

5,317E-6	9,894E-4	5,374E-3	9,9380	25,0	0
3,954E-3	2,149E-3	1,839	20,016	25,0	0
0,01588	4,638E-3	3,424	30,063	25,0	0
0,04142	9,997E-3	4,143	40,141	25,0	0

Stepped flow step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,05286	9,999E-3	5,286	9,9220	25,0	0
0,08218	0,02154	3,815	19,969	25,0	0
0,1096	0,04641	2,362	30,063	25,0	0
0,1399	0,09999	1,400	40,094	25,0	0
0,1233	0,1000	1,233	50,141	25,0	0

Stepped flow step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,05580	0,1000	0,5580	9,9690	25,0	0
0,04075	0,1585	0,2571	20,031	25,0	0
0,03842	0,2512	0,1529	30,047	25,0	0
0,03236	0,3981	0,08129	40,094	25,0	0
0,02906	0,6310	0,04605	50,125	25,0	0
0,02708	1,000	0,02708	60,188	25,0	0

Stepped flow step 4

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,02340	1,000	0,02340	9,9840	25,0	0
0,02505	1,334	0,01878	20,047	25,0	0
0,02586	1,778	0,01454	30,140	25,0	0
0,03355	2,371	0,01415	40,218	25,0	0
0,02805	3,162	8,869E-3	50,281	25,0	0
0,03225	4,217	7,647E-3	60,328	25,0	0
0,04969	5,624	8,835E-3	70,422	25,0	0
0,08971	7,499	0,01196	80,500	25,0	0
0,1730	10,00	0,01730	90,515	25,0	0
0,2922	13,34	0,02191	100,56	25,0	0
0,4135	17,78	0,02325	110,63	25,0	0
0,6233	23,71	0,02628	120,73	25,0	0
0,9923	31,62	0,03138	130,76	25,0	0
1,564	42,17	0,03709	140,89	25,0	0
2,568	56,23	0,04567	150,98	25,0	0
4,198	74,99	0,05599	161,01	25,0	0
6,322	100,0	0,06322	171,13	25,0	0

Temperature ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,1650	10,00	0,01650	9,0000	25,0	0
0,2055	10,00	0,02055	18,012	25,5	0
0,1891	9,998	0,01892	27,004	26,5	0
0,1718	10,00	0,01718	36,008	28,0	0
0,1623	10,00	0,01623	45,004	29,7	0
0,1544	10,00	0,01544	54,008	31,5	0
0,1557	9,998	0,01558	63,000	33,2	0
0,1487	10,00	0,01487	72,016	34,9	0
0,1474	10,00	0,01474	81,008	36,6	0
0,1578	9,991	0,01580	89,996	38,1	0
0,1459	10,00	0,01459	99,004	39,7	0
0,1418	10,00	0,01418	108,00	41,3	0
0,1401	10,00	0,01401	117,02	42,8	0
0,1380	10,00	0,01380	126,00	44,4	0
0,1414	9,999	0,01414	135,01	45,8	0
0,1363	10,00	0,01363	144,00	47,3	0
0,1364	10,00	0,01364	153,00	48,9	0
0,1316	10,00	0,01316	162,01	50,4	0
0,1365	9,999	0,01365	171,01	51,8	0
0,1336	10,00	0,01336	180,00	53,3	0
0,1282	10,00	0,01282	189,02	54,9	0
0,1380	10,00	0,01380	198,02	56,3	0
0,1257	10,00	0,01257	207,02	57,9	0
0,1300	10,00	0,01300	216,01	59,4	0
0,1251	10,00	0,01251	225,01	60,9	0
0,1171	10,00	0,01171	234,00	62,3	0
0,1158	10,00	0,01158	243,00	63,9	0
0,1206	10,00	0,01206	252,00	65,4	0
0,1295	9,999	0,01295	261,01	66,9	0
0,1209	10,00	0,01209	270,01	68,4	0
0,1238	10,00	0,01238	279,00	69,9	0
0,1378	10,00	0,01378	288,01	71,4	0
0,1433	10,00	0,01433	297,00	72,9	0
0,1750	10,00	0,01750	306,00	74,3	0
0,2544	10,00	0,02544	315,01	75,8	0
0,3884	10,00	0,03884	323,99	77,4	0
0,5393	10,00	0,05393	332,99	79,0	0
0,6875	9,999	0,06876	342,00	80,5	0
0,7948	9,999	0,07949	351,01	81,8	0
0,8905	10,00	0,08905	360,01	83,2	0
0,9855	9,999	0,09856	369,00	84,6	0

Temperature ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

1,072	10,00	0,1072	9,0040	86,5	0
1,268	10,00	0,1268	17,996	88,6	0
1,749	9,998	0,1750	27,004	90,2	0
3,409	10,01	0,3405	35,988	91,0	0
3,770	9,999	0,3770	44,992	91,3	0
4,260	10,00	0,4259	53,992	91,3	0
2,829	10,00	0,2829	62,996	91,1	0
2,169	9,987	0,2172	72,008	90,9	0
3,121	9,997	0,3122	80,992	90,7	0
3,049	10,00	0,3049	89,992	90,5	0
2,522	10,00	0,2522	99,000	90,4	0
1,755	10,00	0,1754	108,01	90,3	0
1,366	9,999	0,1366	117,00	90,2	0
1,573	9,997	0,1574	126,00	90,1	0
1,811	9,999	0,1811	135,00	90,1	0
1,489	10,01	0,1487	144,00	90,1	0
1,209	9,998	0,1209	152,99	90,0	0
1,270	10,00	0,1270	161,99	90,0	0
1,113	10,00	0,1113	170,99	90,0	0
1,110	10,00	0,1110	179,99	90,0	0
1,085	10,00	0,1085	189,01	90,0	0
1,073	10,00	0,1073	198,01	90,0	0
1,071	10,00	0,1071	207,00	90,0	0
1,066	10,00	0,1066	216,00	90,0	0
1,054	10,00	0,1054	225,00	90,0	0
1,053	10,00	0,1053	233,99	90,0	0
1,056	9,999	0,1057	242,99	90,0	0
1,040	10,00	0,1040	252,00	90,0	0
1,033	10,00	0,1033	261,00	90,0	0
1,027	10,00	0,1027	270,01	90,0	0
1,026	10,00	0,1026	279,00	90,0	0

Temperature ramp step 3

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

1,020	10,00	0,1020	8,9960	90,0	0
1,013	10,00	0,1013	17,992	89,5	0
0,9999	10,00	0,09999	26,976	86,2	0
0,9958	10,00	0,09958	35,992	85,3	0
0,9959	9,999	0,09960	44,980	84,7	0
1,002	10,00	0,1002	53,984	83,6	0
1,015	10,00	0,1015	62,988	81,2	0
1,031	9,999	0,1032	71,976	79,8	0
1,047	10,00	0,1047	80,976	79,0	0
1,078	10,00	0,1078	89,992	76,6	0
1,072	10,00	0,1072	99,628	75,3	0
1,107	10,00	0,1106	107,99	74,2	0
1,135	10,00	0,1135	116,97	71,8	0
1,146	9,999	0,1146	125,97	71,0	0
1,165	10,00	0,1165	134,98	69,3	0
1,192	10,00	0,1192	143,97	67,4	0
1,194	10,00	0,1194	152,98	66,8	0
1,225	10,00	0,1225	161,98	64,3	0
1,254	10,00	0,1254	170,98	63,5	0
1,268	10,00	0,1268	179,99	61,7	0
1,318	9,998	0,1318	188,99	60,1	0
1,328	9,999	0,1328	197,98	59,1	0
1,372	10,00	0,1372	206,98	56,9	0
1,385	10,00	0,1385	215,98	56,2	0
1,415	10,00	0,1415	224,99	53,9	0
1,467	9,999	0,1467	233,98	52,9	0
1,488	10,00	0,1487	242,98	51,2	0
1,537	10,00	0,1537	251,99	49,7	0
1,615	9,998	0,1615	261,00	48,3	0
1,664	9,999	0,1664	269,99	46,5	0
1,674	10,00	0,1674	279,00	45,5	0
1,724	10,00	0,1724	287,98	43,5	0
1,774	10,00	0,1774	296,99	42,4	0
1,836	10,00	0,1836	305,98	40,6	0
1,946	10,00	0,1946	314,99	39,2	0
1,982	9,998	0,1982	323,98	37,7	0
2,035	10,00	0,2035	332,98	36,2	0
2,075	10,00	0,2074	341,99	34,7	0
2,178	10,00	0,2178	350,99	33,3	0
2,244	10,00	0,2244	359,98	31,8	0
2,304	10,00	0,2304	368,98	30,3	0

Stepped flow step 5

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,02171	1,000E-3	21,70	9,9370	25,1	0
0,05591	2,153E-3	25,97	19,969	24,9	0
0,1072	4,640E-3	23,11	30,031	25,0	0
0,2009	9,999E-3	20,09	40,125	25,1	0

Stepped flow step 6

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,2424	0,01000	24,24	9,9690	25,0	0
0,3095	0,02154	14,37	20,031	24,9	0
0,3722	0,04642	8,018	30,062	25,0	0
0,4570	0,1000	4,570	40,109	25,1	0
0,4668	0,1000	4,668	50,234	25,0	0

Stepped flow step 7

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,5007	0,1000	5,007	9,9530	24,9	0
0,5525	0,1585	3,486	20,000	25,0	0
0,6180	0,2512	2,460	30,031	25,1	0
0,7043	0,3981	1,769	40,047	25,0	0
0,8005	0,6310	1,269	50,125	24,9	0
0,9474	1,000	0,9474	60,172	25,0	0

Stepped flow step 8

shear stress	shear rate	viscosity	time	temperature	normal stress
Pa	1/s	Pa.s	s	C	Pa

0,9411	1,000	0,9411	9,9530	25,1	0
1,051	1,334	0,7879	20,031	25,0	0
1,176	1,778	0,6613	30,141	24,9	0
1,324	2,371	0,5583	40,437	25,0	0
1,535	3,162	0,4853	50,500	25,1	0
1,806	4,217	0,4282	60,578	25,0	0
2,137	5,623	0,3800	70,687	25,0	0
2,518	7,499	0,3358	80,812	25,0	0
2,960	10,00	0,2960	91,047	25,1	0
3,521	13,34	0,2641	101,16	25,0	0
4,217	17,78	0,2371	111,20	25,0	0
5,059	23,71	0,2133	121,25	25,0	0
6,180	31,62	0,1954	131,36	25,0	0
7,852	42,17	0,1862	141,42	25,0	0
10,95	56,23	0,1947	151,52	24,9	0
15,17	74,99	0,2023	161,59	25,0	0
19,81	100,0	0,1981	171,69	25,0	0

